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By: Ethan Gros
Idaho National Laboratory
Idaho Falls, Idaho 83415
http://www.inl.gov
Eddy Current Evaluation Page 2 of 38
ACKNOWLEDGMENTS
This research could not have been possible without the assistance of
Francine Rice, Katelyn Wachs, Adam Robinson, Steve Marschman,
Walter Williams and Michigan State University Professor Dr. Lalita Udpa;
as well as the guidance from my mentor James Smith and the support of
Idaho National Laboratory and the Department of Energy.
Eddy Current Evaluation Page 3 of 38
CONTENTS
1. OBJECTIVE OF EDDY CURRENT TESTING...............................................................7-10
1.1 Calibration ...........................................................................................................7-10
1.1.1 Stage One: Zero Setting ............................................................................7-8
1.1.2 Stage Two: Calibration Setting.................................................................9-10
2. FILM THICKNESSES MEASUREMENT: ACCURACY, REPEATABILITY ..................12-15
2.1 Objective ................................................................................................................12
2.2 Description of Sample.............................................................................................12
2.3 Description of Test Procedure ................................................................................12
2.4 Results & Disscusion.........................................................................................12-14
2.4.1 Day A Test.............................................................................................12-13
2.4.2 Day B Test..................................................................................................14
2.5 Conclusion..............................................................................................................15
3. EFFECT OF PROXIMITYTO EDGE ...........................................................................17-18
3.1 Objective ...............................................................................................................17
3.2 Description of Sample.............................................................................................17
3.3 Description of Test Procedure ...............................................................................17
3.4 Results & Disscusion.........................................................................................17-18
3.5 Conclusion..............................................................................................................18
4. EFFECT OF CONDUCTIVITY OF MATERIALS ...........................................................20-2
4.1 Objective ................................................................................................................20
4.2 Description of Sample.............................................................................................20
4.3 CASE I ..............................................................................................................20-21
4.3.1 Description of Test Procedure................................................................20-21
4.3.2 Results & Disscusion ..................................................................................21
4.3.3 Conclusion..................................................................................................21
4.4 CASE II .............................................................................................................21-26
4.4.1 Description of Test Procedure................................................................21-22
4.4.2 Description of Sample.................................................................................22
4.4.3 Conductivity Test 1 – Materials with similar conductivity ........................22-23
4.4.3.1 Conclusion ..........................................................................................23
4.4.4 Conductivity Test 2 - Day B....................................................................23-24
4.4.4.1 Conclusion ..........................................................................................24
4.4.5 Conductivity Test 3 – Materials with dissimilar conductivity.........................25
4.4.5.1 Description of Test Procedure .............................................................25
4.4.5.2 Conclusion ..........................................................................................25
4.4.6 Conductivity Test 4 – Calibration on Stainless Steel ...................................26
4.4.6.1 Description of Test Procedure .............................................................26
4.4.6.2 Conclusion ..........................................................................................26
Eddy Current Evaluation Page 4 of 38
5. EFFECT OF SURFACE FINISH .................................................................................28-32
5.1 Objective ................................................................................................................28
5.2 Description of Sample.............................................................................................28
5.3 Description of Test Procedure ...........................................................................28-29
5.4 Results & Disscusion.........................................................................................30-31
5.5 Conclusion..............................................................................................................31
5.6 Additional Surface finish Test ............................................................................31-32
5.6.1 Description of Test Procedure.....................................................................31
5.6.2 Results & Disscusion ..................................................................................32
5.6.3 Conclusion..................................................................................................32
6. EFFECT OF CABLE...................................................................................................34-36
6.1 Objective ...............................................................................................................34
6.2 Description of Sample.............................................................................................34
6.3 Description of Test Procedure ...........................................................................34-35
6.4 Results & Disscusion.........................................................................................35-36
6.5 Conclusion..............................................................................................................36
7. RECOMMENDATIONS....................................................................................................38
FIGURES
Figure 1. Front panel of Fischer FMP 40 handle gauge with “Zero” key marked in red................7
Figure 2. Experimental set up showing probe and Al T6 test plate with (a) probe raised
(b) pressed on top of sample. ......................................................................................8
Figure 3. Fischer FMP 40 handle gauge (a) with “10” mark in blue indicates the number
of times the probe was pressed on the Al sample and the “Enter” key marked in
green. (b) Screen with “Normalization finished successfully” message. .......................8
Figure 4. Fischer FMP 40 gauge (a) with the calibration screen up after pressing the
“CAL” button marked in red. (b) the “10” mark in blue which indicates the
number of times the probe was pressed on the Al sample and “Enter” key
marked in green............................................................................................................9
Figure 5. Fischer FMP 40 gauge (a) with the calibration film 1 size (5.46 µm) marked in
teal (b) with “10” mark in blue indicates the number of times the probe was
pressed on the Al sample and “Enter” key marked in green..........................................9
Figure 6. Fischer FMP 40 gauge (a) Fischer FMP 40 gauge (a) with the calibration film 1
size (49.96 µm) marked in teal. (b) the “10” mark in blue which indicates the
number of times the probe was pressed on the Al sample and “Enter” key
marked in green. The message (c) “Corrective Calibration finished
successfully” appears on the screen indicating the calibration was successfully.
...................................................................................................................................10
Figure 7. Fischer Test Films......................................................................................................12
Figure 8. This image is the tip of the eddy current probe next to a ruler. . .................................18
Eddy Current Evaluation Page 5 of 38
Figure 9. These are the two test plates with different surface finishes that were used...............29
Figure 10. This image conveys cable to the eddy current probe coiled......................................34
Figure 11. This image depicts the cable to the eddy current probe kinked. ...............................35
TABLES
Table 1. Mean values of measured thickness along with percent error on Day A......................13
Table 2. Mean values of measured thickness along with percent error on Day B......................14
Table 3. Mean and standard deviation of thickness measured at each (X, Y) position of
probe.…......................................................................................................................17
Table 4. Mean and standard deviation of thickness measured at each (X, Y) position of
probe.…......................................................................................................................18
Table 5. Conductivity values of the alloys used.........................................................................20
Table 6. Mean values of film thickness measured on different alloys. CASE I …. .....................21
Table 7 Conductivity values of the alloys the probe was calibrated on. .…................................22
Table 8 Mean values of thickness measured on each material with different conductivity
value along with percent error. The probe was calibrated on the Al 6061
T6..…. ........................................................................................................................23
Table 9 Mean values of thickness measured on each material with different conductivity
value along with percent error. The probe was calibrated on the Al 6061 T6…...........24
Table 10 Mean values of the measured film on materials with different conductivity
values. The probe was calibrated on Al 6061-T6 plate..…..........................................25
Table 11 Mean values of the measured film thickness on base materials of different
conductivity values. The probe was calibrated on Stainless Steel plate.…..................26
Table 12 Measured values of film thickness on different surface finish along with
standard deviation, and the percent error of measurements. (Actual Value =
77.10 µm)…................................................................................................................30
Table 13 Measured values of film thickness on different surface finish along with
standard deviation, and the percent error of measurements …...................................31
Table 14 Effect of surface finish on film thickness measurement (Actual film thickness in
all cases = 12.22 µm) ….............................................................................................32
Table 15 Case I, II and III results of thickness measurements along with % error.….................36
GRAPH
Graph 1. Conductivity Percent (%) vs Percent Error (%)...... .....................................................24
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1. OBJECTIVE OF EDDY CURRENT TESTING
Eddy-current techniques are widely used in industry to measure the thickness of non-conductive
films on a metal substrate. This is done using a system whereby a coil carrying a high-frequency
alternating current is used to create an alternating magnetic field at the surface of the
instrument's probe. When the probe is brought near a conductive surface, the alternating
magnetic field will induce eddy currents in the conductor. The substrate characteristics and the
distance of the probe from the substrate (the coating thickness) affect the magnitude of the eddy
currents. The induced currents load the probe coil affecting the terminal impedance of the coil.
The measured probe impedance is related to the lift off between coil and conductor as well as
conductivity of the test sample. For a known conductivity sample, the probe impedance can be
converted into an equivalent film thickness value.
The eddy-current test is performed using a commercially available, hand-held eddy-current
probe (ETA3.3H spring-loaded eddy probe running at 8 MHz) that comes with a stand to hold
the probe. The stand holds the probe and adjusts the probe on the z-axis to help position the
probe in the correct area as well as make precise measurements. The signal from the probe is
sent to a hand-held readout, where the results are recorded directly in terms of liftoff or film
thickness.
Understanding the effect of certain factors on the measurements of film thickness, will help to
evaluate how accurate the ETA3.3H spring-loaded eddy probe is at measuring film thickness.
This report documents the results of a study conducted to evaluate the effect of a number of
factors such as i) calibration, ii) conductivity, iii) edge effect iv) surface finish of base material
and v) cable condition.
1.1 CALIBRATION
1.1.1 Stage One: Zero Setting
First the meter readout was set by pressing the button ZERO this sets the thickness of film on
base material as zero(as indicated in Figure 1).
This is the initial
screen after pressing
the “zero” button.
Figure 1. Front panel of Fischer FMP 40 handle gauge with “Zero” key marked in red.
Eddy Current Evaluation Page 8 of 38
The probe was placed in a stand, so the probe was perpendicular to the surface of the metal
test plate. Figure 2(a) shows the initial set up with the Aluminum T6 – Test Plate on the stand.
The lever was pulled in order to lower the probe onto the Aluminum T6 – Test Plate pressing the
probe against the Aluminum Test Plate as indicated in Figure 2(b).
Aluminum T6 – Test Plate
Lever
to
lower
probe
Pressed
probe
The probe was pressed against the plate 10 times (or as many times as the experiments
required) and then ENTER was pressed as indicated in Figure 3(a). When the information is
entered, the message “Normalization finished successfully” appears on the screen indicating
the zero calibration was successfully as indicated in Figure 3(b).
(a) (b)
(a) (b)
Figure 2. Experimental set up showing probe and Al T6 test plate with (a) probe raised (b)
pressed on top of sample.
Figure 3. Fischer FMP 40 handle gauge (a) with “10” mark in blue indicates the
number of times the probe was pressed on the Al sample and the “Enter” key
marked in green. (b) Screen with “Normalization finished successfully” message.
Eddy Current Evaluation Page 9 of 38
1.1.2 Stage Two: Calibration Setting
First the probe was calibrated by pressing the button CAL which starts the calibration process
as indicated in Figure 4(a).The probe was then pressed against the plate 10 times (or as many
times as the experiments required) and ENTER was pressed as indicated in Figure 4(b). A
calibration film 1 of thickness 5.46 µm was then placed on the aluminum plate. Then the output
of the gauge was adjusted according to the known film thickness. Figure 5(a) indicates the
calibration film 1 thickness, which in this case was set to 5.46 µm.
Again probe was pressed against the plate 10 times (or as many times as the experiment
requires) and then ENTER was pressed (as indicated in Figure 5(c)). Figure 6(a) indicates the
calibration film 2 thickness which in this case was 49.96 µm. This film thickness can be varied to
any value. Again probe was pressed against the plate 10 times or as many times as the
experiments require and then ENTER was pressed (as indicated in Figure 6(b)). When the last
10 data points were entered, the message “Corrective Calibration finished successfully”
appears on the screen indicating the calibration was successful (as indicated in Figure 6(c)).
Figure 4. Fischer FMP 40 gauge (a) with the calibration
screen up after pressing the “CAL” button marked in red.
(b) the “10” mark in blue which indicates the number of
times the probe was pressed on the Al sample and
“Enter” key marked in green.
Figure 5. Fischer FMP 40 gauge (a) with the
calibration film 1 size (5.46 µm) marked in
teal (b) with “10” mark in blue indicates the
number of times the probe was pressed on
the Al sample and “Enter” key marked in
green.
Figure 4(a) Figure 4(b) Figure 5(a)
This is the
initial screen
after pressing
the CAL
button.
Eddy Current Evaluation Page 10 of 38
Figure 5(b) Figure 6(a) Figure 6(b) Figure 6(c)
Figure 6. Fischer FMP 40 gauge (a) Fischer FMP 40 gauge (a) with the calibration film 1 size
(49.96 µm) marked in teal. (b) the “10” mark in blue which indicates the number of times the probe
thickness was measured. (c) “Corrective Calibration finished successfully” appears on the screen
Eddy Current Evaluation Page 11 of 38
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2. FILM THICKNESSES MEASUREMENT: ACCURACY, REPEATABILITY
2.1 OBJECTIVE
This section documents the results of thickness measurements on different film thicknesses.
The objective of this experiment was to determine the performance of the instrument in
predicting the thickness of films of known thickness values with respect to accuracy and
repeatability of measurements.
2.2 DESCRIPTION OF SAMPLES.
Different aluminum alloy samples were used as base material in this test to determine the
repeatability and accuracy of the film thickness measurement. The films used in this study were
provided by the Fischer Company as standards and are shown in Figure 7.
Figure 7. Fischer Test Films
The probe was calibrated with a plate of known conductivity and film thicknesses were
measured on the same plate.
2.3 DESCRIPTION OF TEST PROCEDURE
The probe was placed in the stand perpendicular to the surface of a specific Al alloy as the
metal test plate. The probe was then calibrated as described earlier.
Then the probe was used to measure several different film thicknesses on top of the specific
alloy on which the Eddy Current Fischer Probe was calibrated.
2.4 RESULTS & DISCUSSION
2.4.1 Day A Test
The probe measured each film thickness on each alloy three times to get a sample population of
3. Then the three measurements were averaged to get a mean value for each film thickness (as
depicted in Table 1). The percent error was calculated using this formula
|𝐴𝑐𝑡𝑢𝑎𝑙 − 𝑀𝑒𝑎𝑢𝑠𝑢𝑟𝑒𝑑|
𝐴𝑐𝑡𝑢𝑎𝑙
× 100% to
compare the percent error with respect to different film thickness values.
Eddy Current Evaluation Page 13 of 38
Table 1. Mean values of measured thickness along with percent error on Day A.
Key
Percent error 5% or higher
Percent error 15% or higher
Eddy Current Evaluation Page 14 of 38
2.4.2 Day B Test
The probe measured each film on each alloy three times to get a sample population of 3. Then
the three measurements were averaged to get a mean value and percent error for each film
thickness (as depicted in Table 2).
Key
Percent error 5% or higher
Percent error 10% or higher
Percent error 15% or higher
Table 2. Mean values of measured thickness along with percent error on Day B.
Eddy Current Evaluation Page 15 of 38
2.5 CONCLUSION
The data collected on Day A has 6 thickness values that have > 5% error and of these 6 data
points 5 of them are with film thickness < 12.22 µm. Also of these 5 data points 3 of them have
> 15% error. Experiments performed on Day B included additional base material alloys. Data
collected on Day B has 29 thickness values that have > 5% error. Of these 29 points 21 of them
are with film thickness < 12.22 µm. Also there are 14 values that have > 15% error and of these
14 data points 9 are with film of thickness < 5.52 µm and 12 of them are with film of thickness <
12.22 µm.
Therefore it can be concluded that the smaller the film thickness value the larger the percent or
relative error. However, the data is repeatable as long as the probe is calibrated on the same
sample on which the film thickness was measured.
Eddy Current Evaluation Page 16 of 38
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Eddy Current Evaluation Page 17 of 38
3. EFFECT OF PROXIMITY TO EDGE
3.1 OBJECTIVE
This section documents the results of edge effect on eddy current testing. The objective of this
test was to determine whether the proximity of an edge affects the measurements of film
thickness.
3.2 DESCRIPTION OF SAMPLES
This test was performed on Aluminum 6061 T6 – Test Plate. The Eddy Current Fischer Probe
was first calibrated on the same base plate. The test film thickness used was 77.10 µm
3.3 DESCRIPTION OF TEST PROCEDURE
In order to determine the edge effects the probe was first calibrated and placing a film of known
thickness, the experiment consisted of measuring the thickness as the probe was moved from
the middle of the plate out to the edge of the plate.
The probe was moved in the X direction in steps of 5 mm from the center of the test plate
taking 10 data points at each new coordinate (ex. (45,12) (40,12)…) until the probe was
positioned 5 mm from the edge of the test plate (5mm,12mm). The Y-coordinate was kept
constant at 12 mm.
Next, the Y coordinate of probe was varied in steps of 2 mm from the center of the test
plate (ex. (50,10) (50,8)…) until the probe reached 2 mm from the edge of the test plate
(50mm,2mm). The X-coordinate was kept constant at 50 mm.
At each (X,Y) position of the probe, average of 10 measurements values and standard deviation
were calculated. These results are summarized in Table 3 for X direction movement and Table
4 for Y direction movement of the probe.
3.3 RESULTS & DISSCUSSION
Table 3. Mean and standard deviation of thickness measured at each (X, Y) position of probe.
Eddy Current Evaluation Page 18 of 38
3.4 CONCLUSION
The tip of the probe is about 3mm in diameter as indicated in Figure 8 and therefore any data
collected 2mm or 4mm from the edge is likely to be in error as seen in the values measured at
the coordinates (50,4) and (50,2). From the results presented in Tables 3 and 4, it is concluded
that the ETA3.3H spring-loaded eddy current probe is not significantly affected by proximity to
edges as long as the probe is at least 4mm from the edge.
Figure 8. This image is the tip of the eddy current probe next to a ruler.
Table 4. Mean and standard deviation of thickness measured at each (X, Y)
position of probe.
Eddy Current Evaluation Page 19 of 38
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Eddy Current Evaluation Page 20 of 38
4. EFFECT OF CONDUCTIVITY OF MATERIALS
4.1 OBJECTIVE
This section documents the results of thickness measurements using eddy current testing on
materials of conductivity different from that of the calibration sample conductivity. The objective
of this test was to determine whether conductivity of the material affects the measurements of
film thickness.
Two cases were considered as below:
*CASE I: CALIBRATION SAMPLE IS SAME AS SAMPLE USED FOR THICKNESS
MEASUREMENT
*CASE II: CALIBRATION SAMPLE IS DIFFERENT FROM THE SAMPLE USED FOR
THICKNESS MEASUREMENT
4.2 DESCRIPTION OF SAMPLES
In this test we used samples of different conductivity as depicted in Table 5.
Table 5. Conductivity values of the alloys used.
Three different film thicknesses, namely, 11.42 µm, 22.00 µm and 49.54 µm were used to test
the effect of conductivity on thickness measurement.
4.3 CASE I: CALIBRATION SAMPLE IS SAME AS SAMPLE USED FOR THICKNESS
MEASUREMENT
4.3.1 DESCRIPTION OF TEST PROCEDURE
The probe was placed in the stand perpendicular to the surface of the metal test plate. The
probe was then calibrated on a specific sample.
Eddy Current Evaluation Page 21 of 38
The probe was calibrated on each alloy before taking the film thickness measurements. As
described earlier, 10 measurements were taken for each film thickness. These 10
measurements were then averaged to get mean value as shown in Table 6.
4.3.2 RESULTS & DISSCUSION
4.3.3 CASE I: CONCLUSION
The probe produces reasonably accurate measurement of film thicknesses on top of any base
material as long as the probe was calibrated on the same material. The data obtained with
Copper, Tungsten and Stainless steel had higher error in measurement (the data highlighted in
red), however the data variation was about ±0.60 µm and in one extreme case ±0.92 µm, which
translates to 2% or less error.
4.4 CASE II: CALIBRATION SAMPLE IS DIFFERENT FROM THE SAMPLE USED FOR
THICKNESS MEASUREMENT
4.4.1 DESCRIPTION OF TEST PROCEDURE
In this study, the thickness was measured by placing the film on samples of conductivity
different from that of the calibration sample. The Eddy Current Fischer Probe on was calibrated
on a specific material (Aluminum 6061 T6 – Test Plate).
Table 6. Mean values of film thickness measured on different alloys. CASE I
Eddy Current Evaluation Page 22 of 38
Then a specific test film was placed on top of different base material plates and its thickness
was measured to determine whether the conductivity of base material affects the film thickness
measurements.
4.4.2 DESCRIPTION OF SAMPLES
In this test we used samples of different conductivity values as depicted in Table 7.
Table 7. Conductivity values of the alloys the probe was calibrated on.
Five different film thicknesses, namely, 5.52 µm, 11.42 µm, 22.00 µm, 49.54 µm, and 77.10 µm,
were used.
4.4.3 CONDUCTIVITY TEST 1 – Materials with similar conductivity
The probe was calibrated on Aluminum 6061 T6 – Test Plate (row highlighted in green) and
then 10 measurements were taken for the film thickness of 77.10 µm. These 10 measurements
then were averaged to get a mean value of thickness measured on each material with a different
conductivity. The percent error column was calculated using this formula
|𝐴𝑐𝑡𝑢𝑎𝑙 − 𝑀𝑒𝑎𝑢𝑠𝑢𝑟𝑒𝑑|
𝐴𝑐𝑡𝑢𝑎𝑙
× 100% .
Eddy Current Evaluation Page 23 of 38
4.4.3.1 CONCLUSION
Although the conductivity of calibration sample was different from that of the base material used
when measuring the film thickness, there seems to be a large (>4%) error in only two samples,
namely, aluminum 6061 T6511 and Al 6061 Hipped. The conductivity of these two materials
were not available and it is possible that the error is due to difference in conductivity of the
calibration sample and base material.
When there is not a significant change in conductivity values among the materials in table 8
there is not a significant error in thickness values when the probe was calibrated on Al 6061 T6
and thickness is measured on the other alloys .
4.4.4 CONDUCTIVITY TEST 2 – DAY B
The probe was calibrated on Aluminum 6061 T6 – Test Plate with a straight cable (row
highlighted in green) and then 10 measurements were taken for the film thickness of 12.22 µm
and a straight cable. These 10 measurements then were averaged to get a mean values as
conveyed in table 9. The probe was calibrated only on Aluminum 6061 T6 – Test Plate. Then
the 12.22 µm thick film was measured on each of the other alloys.
Table 8. Mean values of thickness measured on base materials with different conductivity value along
with percent error. The probe was calibrated on the Al 6061 T6.
Eddy Current Evaluation Page 24 of 38
4.4.4.1 CONCLUSION
The results in Table 9 are at odds with what was observed earlier. The errors are relative larger
in all these measurements. Some of the base material conductivity values that are largely
different from that of calibration sample are seen to have larger error. However there is no
observable correlation between conductivity difference and error in predicted film thickness.
On the first row, the alloy Al6016-T0 has the largest error namely, 18%, whereas the
conductivity difference between this sample and the calibration sample is roughly 10%. The
randomness of observations in Table 9 is rather troubling and needs to be investigated further.
Table 9. Mean values of thickness measured on each material with different conductivity value
along with percent error. The probe was calibrated on the Al 6061 T6
Graph 1. Conductivity Percent (%) vs Percent Error (%).
Eddy Current Evaluation Page 25 of 38
4.4.5 CONDUCTIVITY TEST 3 – Materials with dissimilar conductivity
4.4.5.1 DESCRIPTION OF TEST PROCEDURE
In this test, the Eddy Current Fischer Probe was calibrated on an Aluminum 6061 T6 – Test
Plate (highlighted). The film thickness was the measured on completely different metals such as
stainless, steel, copper and tungsten. The test film thicknesses used were 11.42 µm, 22.00
µm and 49.54 µm. There were 10 measurements taken for each film thickness. These 10
measurements were then averaged to get a mean value as listed in table 10.
4.4.5.2 CONCLUSION
From Table 10, we observe that the measurements of film thickness on top of copper and the
stainless steel, were in significant error. The stainless steel has lower conductivity value
than that of calibration sample and the measured thickness values were seen to be consistently
larger than the true film thickness. On the other hand copper has a higher conductivity
value than aluminum and the measured thickness values are consistently smaller than the
true film thickness. This is to be expected since higher conductivity value of base material
results in higher eddy current probe signal that can be translated as lower liftoff and hence
smaller film thickness and vice versa.
Table 10. Mean values of the measured film on materials with different conductivity values. The probe
was calibrated on Al 6061-T6 plate.
Eddy Current Evaluation Page 26 of 38
4.4.6 CONDUCTIVITY TEST 4 –Calibration on Stainless Steel
4.4.6.1 DESCRIPTION OF TEST PROCEDURE
In this test, the Eddy Current Fischer Probe was calibrated on a Stainless Steel with
calibrations films of thickness 5.46 µm and 11.42 µm. Then a test film of thickness 5.52 µm
was placed on Al6061-T6 and Copper plates. In each case 10 measurements taken and
averaged to get a mean value as listed in table 11.
4.4.6.2 CONCLUSION
The measurements of film thickness on copper and Al 6061-T6, which both have conductivity
value larger than stainless resulted in negative film thickness output by the instrument, when it
was first calibrated on stainless steel. Therefore it could be hypothesized that if the calibration
sample conductivity is lower than the base material conductivity, the instrument outputs
negative thickness values!! This is clearly a problem with the current instrument.
Table 11. Mean values of the measured film thickness on base materials of different conductivity
values. The probe was calibrated on Stainless Steel plate.
Eddy Current Evaluation Page 27 of 38
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5. EFFECT OF SURFACE FINISH
5.1 OBJECTIVE
This section documents the results of conducting the thickness measurement test on samples
with different surface finishes. The objective of this test was to determine whether the surface
finish affects the measurements of film thickness.
5.2 DESCRIPTION OF SAMPLE
The experiment used two metal test plates. One test plate had six panels with different
machined surface finishes and the second test plate had nine different machined surface
finishes as shown in Figure 9(a) and 9(b).
The G-6 Grit-Blast Microfinish Comparator Surface Roughness Scale (Surface
Roughness Scale) (Figure 9(a)) provides industry with established flat surface roughness
specimens for visual and actual comparison. It is used in specifying and controlling surface
roughness when a product having the appearance of typically machined surfaces is required.
This scale uses a reproduction of accurate machined surfaces measured in microinches. The
numbers engraved alongside each surface are the average deviation from the mean surface
expressed in microinches.
The E-9 Microfinish Comparator Surface Roughness Scale (Microfinish Comparator
Scale) (Figure 9(b)) is made by a dual electroforming process wherein nickel is
electrodeposited to provide an exact reproduction in intricate detail. The surfaces used in this
scale are reproductions of accurately electrical discharge machined surfaces on oil-hardening
tool steel measured in microinches. The numbers engraved alongside each surface are the
average deviation from the mean surface expressed in microinches.
5.3 DESCRIPTION OF TEST PROCEDURE
The probe was placed in the stand perpendicular to the surface of the metal test plate. The
probe was then calibrated on top of the metal test plate on the smoothest surface. This
calibration was done using 22.10 µm and 256.80 µm thick films.
Then a test film of thickness 77.10 µm was placed on top of the lowest surface finish value. The
probe was lowered onto the surface of the plate, so that the probe was completely pressed on
the plate and film thickness was measured. This measurement was repeated 9 times on the
same spot with the same film thickness, so that a total of 10 values were averaged and
recorded. This measurement was repeated with the same film on panels of different surface
finish on the G-6 and E-9 samples.
Eddy Current Evaluation Page 29 of 38
The blue circle represents
the film with the known
thickness 77.10 µm.
The red circle represents
the relative location that
the eddy current probe
touched the surface.
Figure 9 (a & b). These are the
two test plates with different
surface finishes that were used.
Figure 9(a) Figure 9(b)
Eddy Current Evaluation Page 30 of 38
5.4 RESULTS & DISCUSSION
Table 12 presents the mean value of the thickness value obtained with different surface finish in
the two metal test plates. The true film thickness is 77.10 (µm). Also the percent error was
calculated using the formula
|Actual − Meausured|
Actual
× 100% , where “Actual” value is 77.10 µm and
“Measured” is the output of the instrument. The percent error in film thickness measurement for
each surface finish is provided in the last column
Table 13 presents the corresponding film thickness values measured (average of 10
measurements, standard deviation and percent error) on the second metal plate.
Table 12. Measured values of film thickness on different surface finish along with standard
deviation, and the percent error of measurements. (Actual Value = 77.10 µm)
Eddy Current Evaluation Page 31 of 38
5.5 CONCLUSION
The surface finish on which the thickness measurement is made has significant effect on the
output of ETA3.3H eddy probe system. Table 12 indicates that as the surface finish becomes
coarser, the error in measured film thickness value gets larger. Table 13 also indicates that the
error is small for good surface finish and increases with coarser grain finish. Hence, for the
instrument to provide an accurate estimate of the oxide layer thickness, a good surface finish
should be ensured. This conclusion is to be expected since the measurements are made at very
high frequency (8MHz) and eddy current skin depth being very small at this frequency carries
more information on the surface condition. Clearly, the instrument is very sensitive to surface
condition of the sample on which measurement is made.
5.6 ADDITIONAL SURFACE FINISH TEST
5.6.1 DESCRIPTION OF TEST PROCEDURE
In this test, the calibration and film thickness measurement is made on the same panel, i.e. with
the same surface finish.
The Eddy Current Fischer Probe was calibrated on the G-6 Grit-Blast Microfinish Comparator
Surface Roughness Scale (Surface Roughness Scale) at the 32 µin surface finish. A test film
of 12.22 µm thickness was placed on top of the 32 µin surface finish and tested 10 times.
Table 13. Measured values of film thickness on different surface finish along with standard
deviation, and the percent error of measurements
Eddy Current Evaluation Page 32 of 38
Next, the Eddy Current Fischer Probe was re-calibrated on the G-6 Grit-Blast Microfinish
Comparator Surface Roughness Scale at the 1000 µin surface finish. A test film of 12.22 µm
thickness was placed on top of the 1000 µin surface finish value and tested 10 times.
Next, the same two tests were conducted on the E-9 Microfinish Comparator Surface
Roughness Scale (Microfinish Comparator Scale).
The Eddy Current Fischer Probe was calibrated on the E-9 Microfinish Comparator Surface
Roughness Scale at the 16 µin surface finish. A test film of 12.22 µm thickness was placed on
top of the 16 µin surface finish and tested 10 times.
Next, the Eddy Current Fischer Probe was re-calibrated on the E-9 Microfinish Comparator
Surface Roughness Scale at the 250 µin surface finish. A test film of 12.22 µm thickness was
placed on top of the 250 µin surface finish value and tested 10 times.
5.6.2 RESULTS & DISSCUSION
Table 14 presents the 10 measurements values averaged to get a mean value for each surface
finish/ film thickness combination. Also the percent error was calculated using this formula
|Actual − Meausured|
Actual
× 100% to compare the percent error of due to surface finish.
5.6.3 CONCLUSION
The data collected on G-6 Grit-Blast Microfinish Comparator Surface Roughness Scale
supports the idea “that as surface roughness increases, so does the error in film thickness
measurements”.
Table 14. Effect of surface finish on film thickness measurement (Actual film thickness in all cases =
12.22 µm)
Eddy Current Evaluation Page 33 of 38
[This page is meant to be blank]
Eddy Current Evaluation Page 34 of 38
6. EFFECT OF CABLE CONDITION
6.1 OBJECTIVE
This section documents the results of measurements made with a coiled cable. The objective of
this study was to determine whether capacitive effects of coiled cable will affect the performance
of the eddy current probe.
6.2 DESCRIPTION OF SAMPLE
Three different cable configurations were conducted in order to determine whether the cable
effected the film thickness measurements.
6.3 DESCRIPTION OF TEST PROCEDURE
CASE I: COILED CABLE
The probe was placed in the stand perpendicular to the surface of the metal test plate. The
probe was then calibrated on top of a specific alloy.
In order to perform the test the Eddy Current Fischer Probe was calibrated with a straight cable
on a specific material (Aluminum 6061 T6 – Test Plate).
Then the cable was coiled (as depicted in Figure 10) and a specific test film was placed on
base materials with different conductivity values. The test film thickness was then measured
with the eddy current probe.
CASE II: KINKED CABLE
The Eddy Current Fischer Probe was calibrated with a straight cable on Aluminum 6061 T6 –
Test Plate.
Coiled Cable
Figure 10. Eddy current probe measurement with a coiled cable
Eddy Current Evaluation Page 35 of 38
A test film was placed onto materials with different conductivity values. The test film
thickness was then measured with the eddy current probe connected to the “kinked” cable
(as depicted in Figure 10) to determine whether the test film thickness measurement was
affected by the cable configuration.
CASE III: STRAIGHT CABLE
The probe was calibrated on Aluminum 6061 T6 – Test Plate with a straight cable (row
highlighted in green) and then 10 measurements were taken for the film thickness of 12.22 µm
and a straight cable. These 10 measurements then were averaged to get a mean values as
conveyed in table 15. The probe was calibrated only on Aluminum 6061 T6 – Test Plate.
Then the 12.22 µm film was measured on each of the other alloys.
6.4 RESULTS & DISCUSSION
The probe was calibrated on Aluminum 6061 T6 – Test Plate (row highlighted in green). The
test film of true thickness 11.42 µm or 12.22 µm was used on different base materials. 10
measurements were averaged to get mean values as listed in table 15. The percent error (a)
column was calculated using the formula
|𝐴𝑐𝑡𝑢𝑎𝑙 − 𝑀𝑒𝑎𝑢𝑠𝑢𝑟𝑒𝑑|
𝐴𝑐𝑡𝑢𝑎𝑙
× 100% .
Kinked Cable
Figure 10. Eddy current probe measurement with a kinked cable
Eddy Current Evaluation Page 36 of 38
Table 15. Case I, II and III results of thickness measurements along with % error
6.5 CONCLUSION
The results of this study are not very conclusive. There is no clear correlation between the coil
condition and the error in thickness value measured by the instrument. It was expected that the
straight cable would present lowest error in measurement. However, there is no measurable
correlation between the error and cable condition. Further there is also no correlation between
the error in thickness value and base material conductivity.
When the base material is Al6061-T0 tempered alloy, the error in thickness is consistently high.
Although in Table 8, the measurement on Al 6061-T0 produced a small % error. The reason for
this observation needs to be further investigated. At this point, this could be due to repeatability
of performance of the instrument.
Eddy Current Evaluation Page 37 of 38
[This page is meant to be blank]
Eddy Current Evaluation Page 38 of 38
7. RECOMMONDATIONS
In summary, this report documents a study of different parametric effects on film
thickness values measured by the ETA3.3H eddy current probe. The parameters
considered are base material conductivity, edge effect, surface finish and cable
condition. A major problem that was observed is in repeatability of the measurements.
1. The performance of the instrument with respect to edge effect is consistent with
physics of eddy currents. At 8 MHz, the fields are fairly localized and footprint of probe
is very small. Unless the probe is on top of an edge or < 2 mm from edge, the results
are not affected by edge.
2. The effect of surface condition of the material is consistent with physics of eddy
currents. At very high frequency, the probe is very sensitive to surface condition and
hence thickness measurements.
3. The capacitive effects at 8 MHz seems to be much smaller and did not produce
significant error.
4. Conductivity of the calibration sample relative to that of base material is expected to
affect thickness measurement. This was clearly observed when the materials chosen for
calibration is Aluminum alloy and base materials were copper and stainless steel. But
when differently treated alloys of Aluminum were chosen as base material, no
consistent correlation was observable. It is possible that the conductivity values used
from handbook maybe different from true conductivity of the material.
5. Another factor that was not investigated is the effect of temperature. It is well-known
that conductivity of most materials is a function of temperature and hence if we have an
accurate estimate of this dependence and an accurate knowledge of the temperature of
measurement , the effect of temperature can be compensated.

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Eddy Current Evaluation 3-1

  • 1. Eddy Current Evaluation Page 1 of 38 Error! Reference source not found. By: Ethan Gros Idaho National Laboratory Idaho Falls, Idaho 83415 http://www.inl.gov
  • 2. Eddy Current Evaluation Page 2 of 38 ACKNOWLEDGMENTS This research could not have been possible without the assistance of Francine Rice, Katelyn Wachs, Adam Robinson, Steve Marschman, Walter Williams and Michigan State University Professor Dr. Lalita Udpa; as well as the guidance from my mentor James Smith and the support of Idaho National Laboratory and the Department of Energy.
  • 3. Eddy Current Evaluation Page 3 of 38 CONTENTS 1. OBJECTIVE OF EDDY CURRENT TESTING...............................................................7-10 1.1 Calibration ...........................................................................................................7-10 1.1.1 Stage One: Zero Setting ............................................................................7-8 1.1.2 Stage Two: Calibration Setting.................................................................9-10 2. FILM THICKNESSES MEASUREMENT: ACCURACY, REPEATABILITY ..................12-15 2.1 Objective ................................................................................................................12 2.2 Description of Sample.............................................................................................12 2.3 Description of Test Procedure ................................................................................12 2.4 Results & Disscusion.........................................................................................12-14 2.4.1 Day A Test.............................................................................................12-13 2.4.2 Day B Test..................................................................................................14 2.5 Conclusion..............................................................................................................15 3. EFFECT OF PROXIMITYTO EDGE ...........................................................................17-18 3.1 Objective ...............................................................................................................17 3.2 Description of Sample.............................................................................................17 3.3 Description of Test Procedure ...............................................................................17 3.4 Results & Disscusion.........................................................................................17-18 3.5 Conclusion..............................................................................................................18 4. EFFECT OF CONDUCTIVITY OF MATERIALS ...........................................................20-2 4.1 Objective ................................................................................................................20 4.2 Description of Sample.............................................................................................20 4.3 CASE I ..............................................................................................................20-21 4.3.1 Description of Test Procedure................................................................20-21 4.3.2 Results & Disscusion ..................................................................................21 4.3.3 Conclusion..................................................................................................21 4.4 CASE II .............................................................................................................21-26 4.4.1 Description of Test Procedure................................................................21-22 4.4.2 Description of Sample.................................................................................22 4.4.3 Conductivity Test 1 – Materials with similar conductivity ........................22-23 4.4.3.1 Conclusion ..........................................................................................23 4.4.4 Conductivity Test 2 - Day B....................................................................23-24 4.4.4.1 Conclusion ..........................................................................................24 4.4.5 Conductivity Test 3 – Materials with dissimilar conductivity.........................25 4.4.5.1 Description of Test Procedure .............................................................25 4.4.5.2 Conclusion ..........................................................................................25 4.4.6 Conductivity Test 4 – Calibration on Stainless Steel ...................................26 4.4.6.1 Description of Test Procedure .............................................................26 4.4.6.2 Conclusion ..........................................................................................26
  • 4. Eddy Current Evaluation Page 4 of 38 5. EFFECT OF SURFACE FINISH .................................................................................28-32 5.1 Objective ................................................................................................................28 5.2 Description of Sample.............................................................................................28 5.3 Description of Test Procedure ...........................................................................28-29 5.4 Results & Disscusion.........................................................................................30-31 5.5 Conclusion..............................................................................................................31 5.6 Additional Surface finish Test ............................................................................31-32 5.6.1 Description of Test Procedure.....................................................................31 5.6.2 Results & Disscusion ..................................................................................32 5.6.3 Conclusion..................................................................................................32 6. EFFECT OF CABLE...................................................................................................34-36 6.1 Objective ...............................................................................................................34 6.2 Description of Sample.............................................................................................34 6.3 Description of Test Procedure ...........................................................................34-35 6.4 Results & Disscusion.........................................................................................35-36 6.5 Conclusion..............................................................................................................36 7. RECOMMENDATIONS....................................................................................................38 FIGURES Figure 1. Front panel of Fischer FMP 40 handle gauge with “Zero” key marked in red................7 Figure 2. Experimental set up showing probe and Al T6 test plate with (a) probe raised (b) pressed on top of sample. ......................................................................................8 Figure 3. Fischer FMP 40 handle gauge (a) with “10” mark in blue indicates the number of times the probe was pressed on the Al sample and the “Enter” key marked in green. (b) Screen with “Normalization finished successfully” message. .......................8 Figure 4. Fischer FMP 40 gauge (a) with the calibration screen up after pressing the “CAL” button marked in red. (b) the “10” mark in blue which indicates the number of times the probe was pressed on the Al sample and “Enter” key marked in green............................................................................................................9 Figure 5. Fischer FMP 40 gauge (a) with the calibration film 1 size (5.46 µm) marked in teal (b) with “10” mark in blue indicates the number of times the probe was pressed on the Al sample and “Enter” key marked in green..........................................9 Figure 6. Fischer FMP 40 gauge (a) Fischer FMP 40 gauge (a) with the calibration film 1 size (49.96 µm) marked in teal. (b) the “10” mark in blue which indicates the number of times the probe was pressed on the Al sample and “Enter” key marked in green. The message (c) “Corrective Calibration finished successfully” appears on the screen indicating the calibration was successfully. ...................................................................................................................................10 Figure 7. Fischer Test Films......................................................................................................12 Figure 8. This image is the tip of the eddy current probe next to a ruler. . .................................18
  • 5. Eddy Current Evaluation Page 5 of 38 Figure 9. These are the two test plates with different surface finishes that were used...............29 Figure 10. This image conveys cable to the eddy current probe coiled......................................34 Figure 11. This image depicts the cable to the eddy current probe kinked. ...............................35 TABLES Table 1. Mean values of measured thickness along with percent error on Day A......................13 Table 2. Mean values of measured thickness along with percent error on Day B......................14 Table 3. Mean and standard deviation of thickness measured at each (X, Y) position of probe.…......................................................................................................................17 Table 4. Mean and standard deviation of thickness measured at each (X, Y) position of probe.…......................................................................................................................18 Table 5. Conductivity values of the alloys used.........................................................................20 Table 6. Mean values of film thickness measured on different alloys. CASE I …. .....................21 Table 7 Conductivity values of the alloys the probe was calibrated on. .…................................22 Table 8 Mean values of thickness measured on each material with different conductivity value along with percent error. The probe was calibrated on the Al 6061 T6..…. ........................................................................................................................23 Table 9 Mean values of thickness measured on each material with different conductivity value along with percent error. The probe was calibrated on the Al 6061 T6…...........24 Table 10 Mean values of the measured film on materials with different conductivity values. The probe was calibrated on Al 6061-T6 plate..…..........................................25 Table 11 Mean values of the measured film thickness on base materials of different conductivity values. The probe was calibrated on Stainless Steel plate.…..................26 Table 12 Measured values of film thickness on different surface finish along with standard deviation, and the percent error of measurements. (Actual Value = 77.10 µm)…................................................................................................................30 Table 13 Measured values of film thickness on different surface finish along with standard deviation, and the percent error of measurements …...................................31 Table 14 Effect of surface finish on film thickness measurement (Actual film thickness in all cases = 12.22 µm) ….............................................................................................32 Table 15 Case I, II and III results of thickness measurements along with % error.….................36 GRAPH Graph 1. Conductivity Percent (%) vs Percent Error (%)...... .....................................................24
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  • 7. Eddy Current Evaluation Page 7 of 38 1. OBJECTIVE OF EDDY CURRENT TESTING Eddy-current techniques are widely used in industry to measure the thickness of non-conductive films on a metal substrate. This is done using a system whereby a coil carrying a high-frequency alternating current is used to create an alternating magnetic field at the surface of the instrument's probe. When the probe is brought near a conductive surface, the alternating magnetic field will induce eddy currents in the conductor. The substrate characteristics and the distance of the probe from the substrate (the coating thickness) affect the magnitude of the eddy currents. The induced currents load the probe coil affecting the terminal impedance of the coil. The measured probe impedance is related to the lift off between coil and conductor as well as conductivity of the test sample. For a known conductivity sample, the probe impedance can be converted into an equivalent film thickness value. The eddy-current test is performed using a commercially available, hand-held eddy-current probe (ETA3.3H spring-loaded eddy probe running at 8 MHz) that comes with a stand to hold the probe. The stand holds the probe and adjusts the probe on the z-axis to help position the probe in the correct area as well as make precise measurements. The signal from the probe is sent to a hand-held readout, where the results are recorded directly in terms of liftoff or film thickness. Understanding the effect of certain factors on the measurements of film thickness, will help to evaluate how accurate the ETA3.3H spring-loaded eddy probe is at measuring film thickness. This report documents the results of a study conducted to evaluate the effect of a number of factors such as i) calibration, ii) conductivity, iii) edge effect iv) surface finish of base material and v) cable condition. 1.1 CALIBRATION 1.1.1 Stage One: Zero Setting First the meter readout was set by pressing the button ZERO this sets the thickness of film on base material as zero(as indicated in Figure 1). This is the initial screen after pressing the “zero” button. Figure 1. Front panel of Fischer FMP 40 handle gauge with “Zero” key marked in red.
  • 8. Eddy Current Evaluation Page 8 of 38 The probe was placed in a stand, so the probe was perpendicular to the surface of the metal test plate. Figure 2(a) shows the initial set up with the Aluminum T6 – Test Plate on the stand. The lever was pulled in order to lower the probe onto the Aluminum T6 – Test Plate pressing the probe against the Aluminum Test Plate as indicated in Figure 2(b). Aluminum T6 – Test Plate Lever to lower probe Pressed probe The probe was pressed against the plate 10 times (or as many times as the experiments required) and then ENTER was pressed as indicated in Figure 3(a). When the information is entered, the message “Normalization finished successfully” appears on the screen indicating the zero calibration was successfully as indicated in Figure 3(b). (a) (b) (a) (b) Figure 2. Experimental set up showing probe and Al T6 test plate with (a) probe raised (b) pressed on top of sample. Figure 3. Fischer FMP 40 handle gauge (a) with “10” mark in blue indicates the number of times the probe was pressed on the Al sample and the “Enter” key marked in green. (b) Screen with “Normalization finished successfully” message.
  • 9. Eddy Current Evaluation Page 9 of 38 1.1.2 Stage Two: Calibration Setting First the probe was calibrated by pressing the button CAL which starts the calibration process as indicated in Figure 4(a).The probe was then pressed against the plate 10 times (or as many times as the experiments required) and ENTER was pressed as indicated in Figure 4(b). A calibration film 1 of thickness 5.46 µm was then placed on the aluminum plate. Then the output of the gauge was adjusted according to the known film thickness. Figure 5(a) indicates the calibration film 1 thickness, which in this case was set to 5.46 µm. Again probe was pressed against the plate 10 times (or as many times as the experiment requires) and then ENTER was pressed (as indicated in Figure 5(c)). Figure 6(a) indicates the calibration film 2 thickness which in this case was 49.96 µm. This film thickness can be varied to any value. Again probe was pressed against the plate 10 times or as many times as the experiments require and then ENTER was pressed (as indicated in Figure 6(b)). When the last 10 data points were entered, the message “Corrective Calibration finished successfully” appears on the screen indicating the calibration was successful (as indicated in Figure 6(c)). Figure 4. Fischer FMP 40 gauge (a) with the calibration screen up after pressing the “CAL” button marked in red. (b) the “10” mark in blue which indicates the number of times the probe was pressed on the Al sample and “Enter” key marked in green. Figure 5. Fischer FMP 40 gauge (a) with the calibration film 1 size (5.46 µm) marked in teal (b) with “10” mark in blue indicates the number of times the probe was pressed on the Al sample and “Enter” key marked in green. Figure 4(a) Figure 4(b) Figure 5(a) This is the initial screen after pressing the CAL button.
  • 10. Eddy Current Evaluation Page 10 of 38 Figure 5(b) Figure 6(a) Figure 6(b) Figure 6(c) Figure 6. Fischer FMP 40 gauge (a) Fischer FMP 40 gauge (a) with the calibration film 1 size (49.96 µm) marked in teal. (b) the “10” mark in blue which indicates the number of times the probe thickness was measured. (c) “Corrective Calibration finished successfully” appears on the screen
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  • 12. Eddy Current Evaluation Page 12 of 38 2. FILM THICKNESSES MEASUREMENT: ACCURACY, REPEATABILITY 2.1 OBJECTIVE This section documents the results of thickness measurements on different film thicknesses. The objective of this experiment was to determine the performance of the instrument in predicting the thickness of films of known thickness values with respect to accuracy and repeatability of measurements. 2.2 DESCRIPTION OF SAMPLES. Different aluminum alloy samples were used as base material in this test to determine the repeatability and accuracy of the film thickness measurement. The films used in this study were provided by the Fischer Company as standards and are shown in Figure 7. Figure 7. Fischer Test Films The probe was calibrated with a plate of known conductivity and film thicknesses were measured on the same plate. 2.3 DESCRIPTION OF TEST PROCEDURE The probe was placed in the stand perpendicular to the surface of a specific Al alloy as the metal test plate. The probe was then calibrated as described earlier. Then the probe was used to measure several different film thicknesses on top of the specific alloy on which the Eddy Current Fischer Probe was calibrated. 2.4 RESULTS & DISCUSSION 2.4.1 Day A Test The probe measured each film thickness on each alloy three times to get a sample population of 3. Then the three measurements were averaged to get a mean value for each film thickness (as depicted in Table 1). The percent error was calculated using this formula |𝐴𝑐𝑡𝑢𝑎𝑙 − 𝑀𝑒𝑎𝑢𝑠𝑢𝑟𝑒𝑑| 𝐴𝑐𝑡𝑢𝑎𝑙 × 100% to compare the percent error with respect to different film thickness values.
  • 13. Eddy Current Evaluation Page 13 of 38 Table 1. Mean values of measured thickness along with percent error on Day A. Key Percent error 5% or higher Percent error 15% or higher
  • 14. Eddy Current Evaluation Page 14 of 38 2.4.2 Day B Test The probe measured each film on each alloy three times to get a sample population of 3. Then the three measurements were averaged to get a mean value and percent error for each film thickness (as depicted in Table 2). Key Percent error 5% or higher Percent error 10% or higher Percent error 15% or higher Table 2. Mean values of measured thickness along with percent error on Day B.
  • 15. Eddy Current Evaluation Page 15 of 38 2.5 CONCLUSION The data collected on Day A has 6 thickness values that have > 5% error and of these 6 data points 5 of them are with film thickness < 12.22 µm. Also of these 5 data points 3 of them have > 15% error. Experiments performed on Day B included additional base material alloys. Data collected on Day B has 29 thickness values that have > 5% error. Of these 29 points 21 of them are with film thickness < 12.22 µm. Also there are 14 values that have > 15% error and of these 14 data points 9 are with film of thickness < 5.52 µm and 12 of them are with film of thickness < 12.22 µm. Therefore it can be concluded that the smaller the film thickness value the larger the percent or relative error. However, the data is repeatable as long as the probe is calibrated on the same sample on which the film thickness was measured.
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  • 17. Eddy Current Evaluation Page 17 of 38 3. EFFECT OF PROXIMITY TO EDGE 3.1 OBJECTIVE This section documents the results of edge effect on eddy current testing. The objective of this test was to determine whether the proximity of an edge affects the measurements of film thickness. 3.2 DESCRIPTION OF SAMPLES This test was performed on Aluminum 6061 T6 – Test Plate. The Eddy Current Fischer Probe was first calibrated on the same base plate. The test film thickness used was 77.10 µm 3.3 DESCRIPTION OF TEST PROCEDURE In order to determine the edge effects the probe was first calibrated and placing a film of known thickness, the experiment consisted of measuring the thickness as the probe was moved from the middle of the plate out to the edge of the plate. The probe was moved in the X direction in steps of 5 mm from the center of the test plate taking 10 data points at each new coordinate (ex. (45,12) (40,12)…) until the probe was positioned 5 mm from the edge of the test plate (5mm,12mm). The Y-coordinate was kept constant at 12 mm. Next, the Y coordinate of probe was varied in steps of 2 mm from the center of the test plate (ex. (50,10) (50,8)…) until the probe reached 2 mm from the edge of the test plate (50mm,2mm). The X-coordinate was kept constant at 50 mm. At each (X,Y) position of the probe, average of 10 measurements values and standard deviation were calculated. These results are summarized in Table 3 for X direction movement and Table 4 for Y direction movement of the probe. 3.3 RESULTS & DISSCUSSION Table 3. Mean and standard deviation of thickness measured at each (X, Y) position of probe.
  • 18. Eddy Current Evaluation Page 18 of 38 3.4 CONCLUSION The tip of the probe is about 3mm in diameter as indicated in Figure 8 and therefore any data collected 2mm or 4mm from the edge is likely to be in error as seen in the values measured at the coordinates (50,4) and (50,2). From the results presented in Tables 3 and 4, it is concluded that the ETA3.3H spring-loaded eddy current probe is not significantly affected by proximity to edges as long as the probe is at least 4mm from the edge. Figure 8. This image is the tip of the eddy current probe next to a ruler. Table 4. Mean and standard deviation of thickness measured at each (X, Y) position of probe.
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  • 20. Eddy Current Evaluation Page 20 of 38 4. EFFECT OF CONDUCTIVITY OF MATERIALS 4.1 OBJECTIVE This section documents the results of thickness measurements using eddy current testing on materials of conductivity different from that of the calibration sample conductivity. The objective of this test was to determine whether conductivity of the material affects the measurements of film thickness. Two cases were considered as below: *CASE I: CALIBRATION SAMPLE IS SAME AS SAMPLE USED FOR THICKNESS MEASUREMENT *CASE II: CALIBRATION SAMPLE IS DIFFERENT FROM THE SAMPLE USED FOR THICKNESS MEASUREMENT 4.2 DESCRIPTION OF SAMPLES In this test we used samples of different conductivity as depicted in Table 5. Table 5. Conductivity values of the alloys used. Three different film thicknesses, namely, 11.42 µm, 22.00 µm and 49.54 µm were used to test the effect of conductivity on thickness measurement. 4.3 CASE I: CALIBRATION SAMPLE IS SAME AS SAMPLE USED FOR THICKNESS MEASUREMENT 4.3.1 DESCRIPTION OF TEST PROCEDURE The probe was placed in the stand perpendicular to the surface of the metal test plate. The probe was then calibrated on a specific sample.
  • 21. Eddy Current Evaluation Page 21 of 38 The probe was calibrated on each alloy before taking the film thickness measurements. As described earlier, 10 measurements were taken for each film thickness. These 10 measurements were then averaged to get mean value as shown in Table 6. 4.3.2 RESULTS & DISSCUSION 4.3.3 CASE I: CONCLUSION The probe produces reasonably accurate measurement of film thicknesses on top of any base material as long as the probe was calibrated on the same material. The data obtained with Copper, Tungsten and Stainless steel had higher error in measurement (the data highlighted in red), however the data variation was about ±0.60 µm and in one extreme case ±0.92 µm, which translates to 2% or less error. 4.4 CASE II: CALIBRATION SAMPLE IS DIFFERENT FROM THE SAMPLE USED FOR THICKNESS MEASUREMENT 4.4.1 DESCRIPTION OF TEST PROCEDURE In this study, the thickness was measured by placing the film on samples of conductivity different from that of the calibration sample. The Eddy Current Fischer Probe on was calibrated on a specific material (Aluminum 6061 T6 – Test Plate). Table 6. Mean values of film thickness measured on different alloys. CASE I
  • 22. Eddy Current Evaluation Page 22 of 38 Then a specific test film was placed on top of different base material plates and its thickness was measured to determine whether the conductivity of base material affects the film thickness measurements. 4.4.2 DESCRIPTION OF SAMPLES In this test we used samples of different conductivity values as depicted in Table 7. Table 7. Conductivity values of the alloys the probe was calibrated on. Five different film thicknesses, namely, 5.52 µm, 11.42 µm, 22.00 µm, 49.54 µm, and 77.10 µm, were used. 4.4.3 CONDUCTIVITY TEST 1 – Materials with similar conductivity The probe was calibrated on Aluminum 6061 T6 – Test Plate (row highlighted in green) and then 10 measurements were taken for the film thickness of 77.10 µm. These 10 measurements then were averaged to get a mean value of thickness measured on each material with a different conductivity. The percent error column was calculated using this formula |𝐴𝑐𝑡𝑢𝑎𝑙 − 𝑀𝑒𝑎𝑢𝑠𝑢𝑟𝑒𝑑| 𝐴𝑐𝑡𝑢𝑎𝑙 × 100% .
  • 23. Eddy Current Evaluation Page 23 of 38 4.4.3.1 CONCLUSION Although the conductivity of calibration sample was different from that of the base material used when measuring the film thickness, there seems to be a large (>4%) error in only two samples, namely, aluminum 6061 T6511 and Al 6061 Hipped. The conductivity of these two materials were not available and it is possible that the error is due to difference in conductivity of the calibration sample and base material. When there is not a significant change in conductivity values among the materials in table 8 there is not a significant error in thickness values when the probe was calibrated on Al 6061 T6 and thickness is measured on the other alloys . 4.4.4 CONDUCTIVITY TEST 2 – DAY B The probe was calibrated on Aluminum 6061 T6 – Test Plate with a straight cable (row highlighted in green) and then 10 measurements were taken for the film thickness of 12.22 µm and a straight cable. These 10 measurements then were averaged to get a mean values as conveyed in table 9. The probe was calibrated only on Aluminum 6061 T6 – Test Plate. Then the 12.22 µm thick film was measured on each of the other alloys. Table 8. Mean values of thickness measured on base materials with different conductivity value along with percent error. The probe was calibrated on the Al 6061 T6.
  • 24. Eddy Current Evaluation Page 24 of 38 4.4.4.1 CONCLUSION The results in Table 9 are at odds with what was observed earlier. The errors are relative larger in all these measurements. Some of the base material conductivity values that are largely different from that of calibration sample are seen to have larger error. However there is no observable correlation between conductivity difference and error in predicted film thickness. On the first row, the alloy Al6016-T0 has the largest error namely, 18%, whereas the conductivity difference between this sample and the calibration sample is roughly 10%. The randomness of observations in Table 9 is rather troubling and needs to be investigated further. Table 9. Mean values of thickness measured on each material with different conductivity value along with percent error. The probe was calibrated on the Al 6061 T6 Graph 1. Conductivity Percent (%) vs Percent Error (%).
  • 25. Eddy Current Evaluation Page 25 of 38 4.4.5 CONDUCTIVITY TEST 3 – Materials with dissimilar conductivity 4.4.5.1 DESCRIPTION OF TEST PROCEDURE In this test, the Eddy Current Fischer Probe was calibrated on an Aluminum 6061 T6 – Test Plate (highlighted). The film thickness was the measured on completely different metals such as stainless, steel, copper and tungsten. The test film thicknesses used were 11.42 µm, 22.00 µm and 49.54 µm. There were 10 measurements taken for each film thickness. These 10 measurements were then averaged to get a mean value as listed in table 10. 4.4.5.2 CONCLUSION From Table 10, we observe that the measurements of film thickness on top of copper and the stainless steel, were in significant error. The stainless steel has lower conductivity value than that of calibration sample and the measured thickness values were seen to be consistently larger than the true film thickness. On the other hand copper has a higher conductivity value than aluminum and the measured thickness values are consistently smaller than the true film thickness. This is to be expected since higher conductivity value of base material results in higher eddy current probe signal that can be translated as lower liftoff and hence smaller film thickness and vice versa. Table 10. Mean values of the measured film on materials with different conductivity values. The probe was calibrated on Al 6061-T6 plate.
  • 26. Eddy Current Evaluation Page 26 of 38 4.4.6 CONDUCTIVITY TEST 4 –Calibration on Stainless Steel 4.4.6.1 DESCRIPTION OF TEST PROCEDURE In this test, the Eddy Current Fischer Probe was calibrated on a Stainless Steel with calibrations films of thickness 5.46 µm and 11.42 µm. Then a test film of thickness 5.52 µm was placed on Al6061-T6 and Copper plates. In each case 10 measurements taken and averaged to get a mean value as listed in table 11. 4.4.6.2 CONCLUSION The measurements of film thickness on copper and Al 6061-T6, which both have conductivity value larger than stainless resulted in negative film thickness output by the instrument, when it was first calibrated on stainless steel. Therefore it could be hypothesized that if the calibration sample conductivity is lower than the base material conductivity, the instrument outputs negative thickness values!! This is clearly a problem with the current instrument. Table 11. Mean values of the measured film thickness on base materials of different conductivity values. The probe was calibrated on Stainless Steel plate.
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  • 28. Eddy Current Evaluation Page 28 of 38 5. EFFECT OF SURFACE FINISH 5.1 OBJECTIVE This section documents the results of conducting the thickness measurement test on samples with different surface finishes. The objective of this test was to determine whether the surface finish affects the measurements of film thickness. 5.2 DESCRIPTION OF SAMPLE The experiment used two metal test plates. One test plate had six panels with different machined surface finishes and the second test plate had nine different machined surface finishes as shown in Figure 9(a) and 9(b). The G-6 Grit-Blast Microfinish Comparator Surface Roughness Scale (Surface Roughness Scale) (Figure 9(a)) provides industry with established flat surface roughness specimens for visual and actual comparison. It is used in specifying and controlling surface roughness when a product having the appearance of typically machined surfaces is required. This scale uses a reproduction of accurate machined surfaces measured in microinches. The numbers engraved alongside each surface are the average deviation from the mean surface expressed in microinches. The E-9 Microfinish Comparator Surface Roughness Scale (Microfinish Comparator Scale) (Figure 9(b)) is made by a dual electroforming process wherein nickel is electrodeposited to provide an exact reproduction in intricate detail. The surfaces used in this scale are reproductions of accurately electrical discharge machined surfaces on oil-hardening tool steel measured in microinches. The numbers engraved alongside each surface are the average deviation from the mean surface expressed in microinches. 5.3 DESCRIPTION OF TEST PROCEDURE The probe was placed in the stand perpendicular to the surface of the metal test plate. The probe was then calibrated on top of the metal test plate on the smoothest surface. This calibration was done using 22.10 µm and 256.80 µm thick films. Then a test film of thickness 77.10 µm was placed on top of the lowest surface finish value. The probe was lowered onto the surface of the plate, so that the probe was completely pressed on the plate and film thickness was measured. This measurement was repeated 9 times on the same spot with the same film thickness, so that a total of 10 values were averaged and recorded. This measurement was repeated with the same film on panels of different surface finish on the G-6 and E-9 samples.
  • 29. Eddy Current Evaluation Page 29 of 38 The blue circle represents the film with the known thickness 77.10 µm. The red circle represents the relative location that the eddy current probe touched the surface. Figure 9 (a & b). These are the two test plates with different surface finishes that were used. Figure 9(a) Figure 9(b)
  • 30. Eddy Current Evaluation Page 30 of 38 5.4 RESULTS & DISCUSSION Table 12 presents the mean value of the thickness value obtained with different surface finish in the two metal test plates. The true film thickness is 77.10 (µm). Also the percent error was calculated using the formula |Actual − Meausured| Actual × 100% , where “Actual” value is 77.10 µm and “Measured” is the output of the instrument. The percent error in film thickness measurement for each surface finish is provided in the last column Table 13 presents the corresponding film thickness values measured (average of 10 measurements, standard deviation and percent error) on the second metal plate. Table 12. Measured values of film thickness on different surface finish along with standard deviation, and the percent error of measurements. (Actual Value = 77.10 µm)
  • 31. Eddy Current Evaluation Page 31 of 38 5.5 CONCLUSION The surface finish on which the thickness measurement is made has significant effect on the output of ETA3.3H eddy probe system. Table 12 indicates that as the surface finish becomes coarser, the error in measured film thickness value gets larger. Table 13 also indicates that the error is small for good surface finish and increases with coarser grain finish. Hence, for the instrument to provide an accurate estimate of the oxide layer thickness, a good surface finish should be ensured. This conclusion is to be expected since the measurements are made at very high frequency (8MHz) and eddy current skin depth being very small at this frequency carries more information on the surface condition. Clearly, the instrument is very sensitive to surface condition of the sample on which measurement is made. 5.6 ADDITIONAL SURFACE FINISH TEST 5.6.1 DESCRIPTION OF TEST PROCEDURE In this test, the calibration and film thickness measurement is made on the same panel, i.e. with the same surface finish. The Eddy Current Fischer Probe was calibrated on the G-6 Grit-Blast Microfinish Comparator Surface Roughness Scale (Surface Roughness Scale) at the 32 µin surface finish. A test film of 12.22 µm thickness was placed on top of the 32 µin surface finish and tested 10 times. Table 13. Measured values of film thickness on different surface finish along with standard deviation, and the percent error of measurements
  • 32. Eddy Current Evaluation Page 32 of 38 Next, the Eddy Current Fischer Probe was re-calibrated on the G-6 Grit-Blast Microfinish Comparator Surface Roughness Scale at the 1000 µin surface finish. A test film of 12.22 µm thickness was placed on top of the 1000 µin surface finish value and tested 10 times. Next, the same two tests were conducted on the E-9 Microfinish Comparator Surface Roughness Scale (Microfinish Comparator Scale). The Eddy Current Fischer Probe was calibrated on the E-9 Microfinish Comparator Surface Roughness Scale at the 16 µin surface finish. A test film of 12.22 µm thickness was placed on top of the 16 µin surface finish and tested 10 times. Next, the Eddy Current Fischer Probe was re-calibrated on the E-9 Microfinish Comparator Surface Roughness Scale at the 250 µin surface finish. A test film of 12.22 µm thickness was placed on top of the 250 µin surface finish value and tested 10 times. 5.6.2 RESULTS & DISSCUSION Table 14 presents the 10 measurements values averaged to get a mean value for each surface finish/ film thickness combination. Also the percent error was calculated using this formula |Actual − Meausured| Actual × 100% to compare the percent error of due to surface finish. 5.6.3 CONCLUSION The data collected on G-6 Grit-Blast Microfinish Comparator Surface Roughness Scale supports the idea “that as surface roughness increases, so does the error in film thickness measurements”. Table 14. Effect of surface finish on film thickness measurement (Actual film thickness in all cases = 12.22 µm)
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  • 34. Eddy Current Evaluation Page 34 of 38 6. EFFECT OF CABLE CONDITION 6.1 OBJECTIVE This section documents the results of measurements made with a coiled cable. The objective of this study was to determine whether capacitive effects of coiled cable will affect the performance of the eddy current probe. 6.2 DESCRIPTION OF SAMPLE Three different cable configurations were conducted in order to determine whether the cable effected the film thickness measurements. 6.3 DESCRIPTION OF TEST PROCEDURE CASE I: COILED CABLE The probe was placed in the stand perpendicular to the surface of the metal test plate. The probe was then calibrated on top of a specific alloy. In order to perform the test the Eddy Current Fischer Probe was calibrated with a straight cable on a specific material (Aluminum 6061 T6 – Test Plate). Then the cable was coiled (as depicted in Figure 10) and a specific test film was placed on base materials with different conductivity values. The test film thickness was then measured with the eddy current probe. CASE II: KINKED CABLE The Eddy Current Fischer Probe was calibrated with a straight cable on Aluminum 6061 T6 – Test Plate. Coiled Cable Figure 10. Eddy current probe measurement with a coiled cable
  • 35. Eddy Current Evaluation Page 35 of 38 A test film was placed onto materials with different conductivity values. The test film thickness was then measured with the eddy current probe connected to the “kinked” cable (as depicted in Figure 10) to determine whether the test film thickness measurement was affected by the cable configuration. CASE III: STRAIGHT CABLE The probe was calibrated on Aluminum 6061 T6 – Test Plate with a straight cable (row highlighted in green) and then 10 measurements were taken for the film thickness of 12.22 µm and a straight cable. These 10 measurements then were averaged to get a mean values as conveyed in table 15. The probe was calibrated only on Aluminum 6061 T6 – Test Plate. Then the 12.22 µm film was measured on each of the other alloys. 6.4 RESULTS & DISCUSSION The probe was calibrated on Aluminum 6061 T6 – Test Plate (row highlighted in green). The test film of true thickness 11.42 µm or 12.22 µm was used on different base materials. 10 measurements were averaged to get mean values as listed in table 15. The percent error (a) column was calculated using the formula |𝐴𝑐𝑡𝑢𝑎𝑙 − 𝑀𝑒𝑎𝑢𝑠𝑢𝑟𝑒𝑑| 𝐴𝑐𝑡𝑢𝑎𝑙 × 100% . Kinked Cable Figure 10. Eddy current probe measurement with a kinked cable
  • 36. Eddy Current Evaluation Page 36 of 38 Table 15. Case I, II and III results of thickness measurements along with % error 6.5 CONCLUSION The results of this study are not very conclusive. There is no clear correlation between the coil condition and the error in thickness value measured by the instrument. It was expected that the straight cable would present lowest error in measurement. However, there is no measurable correlation between the error and cable condition. Further there is also no correlation between the error in thickness value and base material conductivity. When the base material is Al6061-T0 tempered alloy, the error in thickness is consistently high. Although in Table 8, the measurement on Al 6061-T0 produced a small % error. The reason for this observation needs to be further investigated. At this point, this could be due to repeatability of performance of the instrument.
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  • 38. Eddy Current Evaluation Page 38 of 38 7. RECOMMONDATIONS In summary, this report documents a study of different parametric effects on film thickness values measured by the ETA3.3H eddy current probe. The parameters considered are base material conductivity, edge effect, surface finish and cable condition. A major problem that was observed is in repeatability of the measurements. 1. The performance of the instrument with respect to edge effect is consistent with physics of eddy currents. At 8 MHz, the fields are fairly localized and footprint of probe is very small. Unless the probe is on top of an edge or < 2 mm from edge, the results are not affected by edge. 2. The effect of surface condition of the material is consistent with physics of eddy currents. At very high frequency, the probe is very sensitive to surface condition and hence thickness measurements. 3. The capacitive effects at 8 MHz seems to be much smaller and did not produce significant error. 4. Conductivity of the calibration sample relative to that of base material is expected to affect thickness measurement. This was clearly observed when the materials chosen for calibration is Aluminum alloy and base materials were copper and stainless steel. But when differently treated alloys of Aluminum were chosen as base material, no consistent correlation was observable. It is possible that the conductivity values used from handbook maybe different from true conductivity of the material. 5. Another factor that was not investigated is the effect of temperature. It is well-known that conductivity of most materials is a function of temperature and hence if we have an accurate estimate of this dependence and an accurate knowledge of the temperature of measurement , the effect of temperature can be compensated.