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Standardization of Acids and bases. 2. Determination of pKa and pKb values 3. Preparation of solutions of different pH & buffer capacities. 4. Determination of phase diagram of binary systems. Determination of distribution coefficients. 6. Determination of molecular weight by Victor Meyer’s Method. 7. Determination of heats of solutions by measuring solubility as a function of temperature (Van’t Hoff equation.)
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A. Qualitative analysis of metal ions and acid radicals: Na+, K+, Ca+2, Ag+, Mn+4, Fe+2, Fe+3, Co+2, Mg+2, Al+3, Cu+2 and acid radicals CO3, halides, Citrate SO4-2, NO3-, SO3-2, etc. B. Identification of inorganic drugs in their formulation: 1. Ca+2, from supplied preparations 2. Fe+2 from supplied preparations 3. Al+3 from supplied preparations 4. Mg+2 from supplied preparations 5. K+ from supplied reparations 6. Na+ from supplied preparations C. Conversion of different water insoluble or sparingly soluble drugs into water soluble forms: 1. Na/ K – salicylate from salicylic acid 2. Na/ K – benzoate from benzoic acid 3. Na/ K – citrate from citric acid
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Standardization of Acids and bases. 2. Determination of pKa and pKb values 3. Preparation of solutions of different pH & buffer capacities. 4. Determination of phase diagram of binary systems. Determination of distribution coefficients. 6. Determination of molecular weight by Victor Meyer’s Method. 7. Determination of heats of solutions by measuring solubility as a function of temperature (Van’t Hoff equation.)
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A. Qualitative analysis of metal ions and acid radicals: Na+, K+, Ca+2, Ag+, Mn+4, Fe+2, Fe+3, Co+2, Mg+2, Al+3, Cu+2 and acid radicals CO3, halides, Citrate SO4-2, NO3-, SO3-2, etc. B. Identification of inorganic drugs in their formulation: 1. Ca+2, from supplied preparations 2. Fe+2 from supplied preparations 3. Al+3 from supplied preparations 4. Mg+2 from supplied preparations 5. K+ from supplied reparations 6. Na+ from supplied preparations C. Conversion of different water insoluble or sparingly soluble drugs into water soluble forms: 1. Na/ K – salicylate from salicylic acid 2. Na/ K – benzoate from benzoic acid 3. Na/ K – citrate from citric acid
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Plant analysis: Extraction, separation, chromatography, types of plant constituents, comparative phytochemistry and chemotaxonomy.
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Structure of the cell as a unit: Its function and form. Introduction to general structure of the morphological parts of plants.
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Crude drugs: A general view of their origin, distributions, cultivation, collection, drying and storage, commerce and quality control. a) Classification of drugs. b) Preparation of drugs for commercial market c) Evaluation of crude drugs. d) Drug adulteration.
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Resin and resin combinations: Resin, oleo-resin, oleo-gum resin, tolu balsam and benzoin.
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Poisonous plants and natural pesticides: Datura, poison hemlock, water hemlock, foxglove (digitalis). Ipornoca, tobbaco, poppy, pyrethrum flower, Derris & Ianchocarpus, red squill, strychnine, etc.
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lycosides and glycoside containing drugs. Biosynthesis of glycosides: The details of the followings: i) Cyanogenic: Wild Cherry ii)Isothiocyanate-Mustard (Black mustard and white mustard). iii) Cardiac: Digitalis, strophanthus, squill. B.Pharm Syllabus Northern University Bangladesh De ve loped b y: Ma hab ur R a hma n She i kh & M ahm ud ur R ahman Assistant Professors, Department of Pharmacy, Northern University Bangladesh 30 iv) Saponins: Sarsaparilla, glycyrrhiza, dioscorea. v) Anthraquinone glycosides: Cascara sagrada, aloe, senna, rhubarb. vi) Other glycosides and neutral principles: Gentian, quassia, saffron.
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Alkaloids: The details of the followings: Biosynthesis of tropane, quinoline, isoquinoline and indole alkaloids. i) Tropane-Belladona, stramonium, hyoscyamus and lica ii)Quinoline-Cinchona, Cusparia bark iii) Isoquinoline-Ipecacs, Opium, sanguinaria, curare iv) Indole-Rawolfia, Nux vomica, Ergot, Catharanthus v) Imidazole: Pilocarpine vi) Steroidal: Veretrum viride, aconite vii)Lupinea-Lupinus spp viii) Purine base-Coffee, tea.
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