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4th Meeting of the Global Soil Laboratory Network (GLOSOLAN)
Ms. Lucrezia Caon
GLOSOLAN Coordinator
Item 19
Endorsement of the GLOSOLAN SOPs
2019-2020 and discussion on the SOPs
review procedure
4th Meeting of the Global Soil Laboratory Network (GLOSOLAN)
Quick recap on how GLOSOLAN SOPs are prepared
1. RESOLANs express an opinion on the SOPs they would like GLOSOLAN to
harmonize
2. A decision on the SOPs to harmonize is made at the annual GLOSOLAN meeting
based on the proposals made by RESOLANs
3. Identification of regional leaders and establishment of the working groups (1
per each SOP).
Regional leaders should:
- Contribute to prepare the SOP matrix
4th Meeting of the Global Soil Laboratory Network (GLOSOLAN)
4th Meeting of the Global Soil Laboratory Network (GLOSOLAN)
Quick recap on how GLOSOLAN SOPs are prepared
1. RESOLANs express an opinion on the SOPs they would like GLOSOLAN to
harmonize
2. A decision on the SOPs to harmonize is made at the annual GLOSOLAN meeting
based on the proposals made by RESOLANs
3. Identification of regional leaders and establishment of the working groups (1
per each SOP).
Regional leaders should:
- Contribute to prepare the SOP matrix
- Harmonize the information in the matrix for their region
4th Meeting of the Global Soil Laboratory Network (GLOSOLAN)
4th Meeting of the Global Soil Laboratory Network (GLOSOLAN)
Quick recap on how GLOSOLAN SOPs are prepared
1. RESOLANs express an opinion on the SOPs they would like GLOSOLAN to
harmonize
2. A decision on the SOPs to harmonize is made at the annual GLOSOLAN meeting
based on the proposals made by RESOLANs
3. Identification of regional leaders and establishment of the working groups (1
per each SOP).
Regional leaders should:
- Contribute to prepare the SOP matrix
- Harmonize the information in the matrix for their region
- Contribute to the global harmonization of information
- Draft/review/finalize the GLOSOLAN SOP
Each SOP has a regional leader serving as global leader too. The global leader takes
the overall responsibility for the writing of the SOP
4th Meeting of the Global Soil Laboratory Network (GLOSOLAN)
All laboratories sending information and all authors
are acknowledged in the GLOSOLAN SOPs
4th Meeting of the Global Soil Laboratory Network (GLOSOLAN)
All laboratories sending information and all authors
are acknowledged in the GLOSOLAN SOPs
4th Meeting of the Global Soil Laboratory Network (GLOSOLAN)
Code SOP Version Effective data
GLOSOLAN-SOP-01 Handling and preparation of soil
samples for chemical and physical
analysis
2 28 October 2019
GLOSOLAN-SOP-02 Soil organic carbon Walkley and Black
– titration and colorimetric method
2 28 October 2019
GLOSOLAN-SOP-03 Soil total carbon – Dumas dry
combustion method
2 28 October 2019
GLOSOLAN-SOP-04 Soil calcium carbonate equivalent –
volumetric calcimeter method
2 28 October 2019
GLOSOLAN-SOP-05 Soil calcium carbonate equivalent –
titrimetric method
2 28 October 2019
SOPs harmonized in 2018-2019
Final review and endorsement at the 3rd GLOSOLAN meeting
These SOPs will be updated with
the units of measure we agreed
upon yesterday
4th Meeting of the Global Soil Laboratory Network (GLOSOLAN)
Code SOP Version Effective data
GLOSOLAN-SOP-06 Soil pH determination 1
GLOSOLAN-SOP-07 Soil Electrical Conductivity
(soil/water, 1:5)
1
GLOSOLAN-SOP-08 Saturated soil paste extract 1
GLOSOLAN-SOP-09 Soil Available Phosphorous Bray I and
II Methods
1
GLOSOLAN-SOP-10 Soil Available Phosphorous – Olsen
method
1
GLOSOLAN-SOP-11 Soil available phosphorous - Mehlich I
Method
1
SOPs harmonized in 2019-2020
4th Meeting of the Global Soil Laboratory Network (GLOSOLAN)
Code SOP Version Effective data
GLOSOLAN-SOP-12 Mehlich III
GLOSOLAN-SOP-13 Soil total nitrogen – Dumas dry
combustion method
1
GLOSOLAN-SOP-14 Soil Nitrogen – Kjeldahl method 1
GLOSOLAN-SOP-15 Mineral N
GLOSOLAN-SOP-16 Soil organic carbon – Tyurin
colorimetric method
1
SOPs harmonized in 2019-2020
4th Meeting of the Global Soil Laboratory Network (GLOSOLAN)
The draft of all SOPs were sent to:
- National reference laboratories
- Laboratories that completed the input matrixes
for review
Working groups compiled and addressed the feedbacks received
by reviewers but noticed that:
1. Many reviewers ignored the fact that the GLOSOLAN SOPs are
the result of a harmonization process. Reviews referred to the
procedures their labs are currently implementing
2. Draft SOPs are taken for final SOPs. Some labs started to
implement them already
4th Meeting of the Global Soil Laboratory Network (GLOSOLAN)
As per the decisions we made on Wednesday, a
Review Panel (1 per SOP) will do the final
review and endorsement of these SOPs
Proposal:
The GLOSOLAN coordinator and the SOP’s global leader
will select a few experts to join the Review Panel. Experts will be
identified based on the quality of the reviews they sent
Poll
4th Meeting of the Global Soil Laboratory Network (GLOSOLAN)
Thanks for your contribution!

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Item 19. Endorsement of the GLOSOLAN SOPs 2019-2020 and discussion on the SOPs review procedure

  • 1. 4th Meeting of the Global Soil Laboratory Network (GLOSOLAN) Ms. Lucrezia Caon GLOSOLAN Coordinator Item 19 Endorsement of the GLOSOLAN SOPs 2019-2020 and discussion on the SOPs review procedure
  • 2. 4th Meeting of the Global Soil Laboratory Network (GLOSOLAN) Quick recap on how GLOSOLAN SOPs are prepared 1. RESOLANs express an opinion on the SOPs they would like GLOSOLAN to harmonize 2. A decision on the SOPs to harmonize is made at the annual GLOSOLAN meeting based on the proposals made by RESOLANs 3. Identification of regional leaders and establishment of the working groups (1 per each SOP). Regional leaders should: - Contribute to prepare the SOP matrix
  • 3. 4th Meeting of the Global Soil Laboratory Network (GLOSOLAN)
  • 4. 4th Meeting of the Global Soil Laboratory Network (GLOSOLAN) Quick recap on how GLOSOLAN SOPs are prepared 1. RESOLANs express an opinion on the SOPs they would like GLOSOLAN to harmonize 2. A decision on the SOPs to harmonize is made at the annual GLOSOLAN meeting based on the proposals made by RESOLANs 3. Identification of regional leaders and establishment of the working groups (1 per each SOP). Regional leaders should: - Contribute to prepare the SOP matrix - Harmonize the information in the matrix for their region
  • 5. 4th Meeting of the Global Soil Laboratory Network (GLOSOLAN)
  • 6. 4th Meeting of the Global Soil Laboratory Network (GLOSOLAN) Quick recap on how GLOSOLAN SOPs are prepared 1. RESOLANs express an opinion on the SOPs they would like GLOSOLAN to harmonize 2. A decision on the SOPs to harmonize is made at the annual GLOSOLAN meeting based on the proposals made by RESOLANs 3. Identification of regional leaders and establishment of the working groups (1 per each SOP). Regional leaders should: - Contribute to prepare the SOP matrix - Harmonize the information in the matrix for their region - Contribute to the global harmonization of information - Draft/review/finalize the GLOSOLAN SOP Each SOP has a regional leader serving as global leader too. The global leader takes the overall responsibility for the writing of the SOP
  • 7. 4th Meeting of the Global Soil Laboratory Network (GLOSOLAN) All laboratories sending information and all authors are acknowledged in the GLOSOLAN SOPs
  • 8. 4th Meeting of the Global Soil Laboratory Network (GLOSOLAN) All laboratories sending information and all authors are acknowledged in the GLOSOLAN SOPs
  • 9. 4th Meeting of the Global Soil Laboratory Network (GLOSOLAN) Code SOP Version Effective data GLOSOLAN-SOP-01 Handling and preparation of soil samples for chemical and physical analysis 2 28 October 2019 GLOSOLAN-SOP-02 Soil organic carbon Walkley and Black – titration and colorimetric method 2 28 October 2019 GLOSOLAN-SOP-03 Soil total carbon – Dumas dry combustion method 2 28 October 2019 GLOSOLAN-SOP-04 Soil calcium carbonate equivalent – volumetric calcimeter method 2 28 October 2019 GLOSOLAN-SOP-05 Soil calcium carbonate equivalent – titrimetric method 2 28 October 2019 SOPs harmonized in 2018-2019 Final review and endorsement at the 3rd GLOSOLAN meeting These SOPs will be updated with the units of measure we agreed upon yesterday
  • 10. 4th Meeting of the Global Soil Laboratory Network (GLOSOLAN) Code SOP Version Effective data GLOSOLAN-SOP-06 Soil pH determination 1 GLOSOLAN-SOP-07 Soil Electrical Conductivity (soil/water, 1:5) 1 GLOSOLAN-SOP-08 Saturated soil paste extract 1 GLOSOLAN-SOP-09 Soil Available Phosphorous Bray I and II Methods 1 GLOSOLAN-SOP-10 Soil Available Phosphorous – Olsen method 1 GLOSOLAN-SOP-11 Soil available phosphorous - Mehlich I Method 1 SOPs harmonized in 2019-2020
  • 11. 4th Meeting of the Global Soil Laboratory Network (GLOSOLAN) Code SOP Version Effective data GLOSOLAN-SOP-12 Mehlich III GLOSOLAN-SOP-13 Soil total nitrogen – Dumas dry combustion method 1 GLOSOLAN-SOP-14 Soil Nitrogen – Kjeldahl method 1 GLOSOLAN-SOP-15 Mineral N GLOSOLAN-SOP-16 Soil organic carbon – Tyurin colorimetric method 1 SOPs harmonized in 2019-2020
  • 12. 4th Meeting of the Global Soil Laboratory Network (GLOSOLAN) The draft of all SOPs were sent to: - National reference laboratories - Laboratories that completed the input matrixes for review Working groups compiled and addressed the feedbacks received by reviewers but noticed that: 1. Many reviewers ignored the fact that the GLOSOLAN SOPs are the result of a harmonization process. Reviews referred to the procedures their labs are currently implementing 2. Draft SOPs are taken for final SOPs. Some labs started to implement them already
  • 13. 4th Meeting of the Global Soil Laboratory Network (GLOSOLAN) As per the decisions we made on Wednesday, a Review Panel (1 per SOP) will do the final review and endorsement of these SOPs Proposal: The GLOSOLAN coordinator and the SOP’s global leader will select a few experts to join the Review Panel. Experts will be identified based on the quality of the reviews they sent Poll
  • 14. 4th Meeting of the Global Soil Laboratory Network (GLOSOLAN) Thanks for your contribution!