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Do Kyung Kim Department of Materials Science and Engineering KAIST, Korea Nanoindentation Lecture 2 Case Study
Applications of nanoindentation ,[object Object],[object Object],[object Object],[object Object],[object Object]
Mechanical Characterization  of Nanostructures
Carbon Nanotube (1) ,[object Object],[object Object],Sample A Sample B Sample C Gleason, J Mech Phys Solids, 2003
Carbon Nanotube (2) ,[object Object],[object Object],Gleason, J Mech Phys Solids, 2003
Carbon Nanotube (2) ,[object Object],[object Object],Gleason, J Mech Phys Solids, 2003
Silver Nanowire (1) ,[object Object],[object Object],[object Object],Caswell, Nano Letters, 2003
Silver Nanowire (2) ,[object Object],[object Object],[object Object],Caswell, Nano Letters, 2003
ZnO and SnO2 nanobelt (1) ,[object Object],[object Object],Wang, APL, 2003
ZnO and SnO2 nanobelt (2) ,[object Object],[object Object],Wang, APL, 2003
Pressure-induced Phase Transformation
Silicon (1) ,[object Object],[object Object],[object Object],Gogotsi, J Mater Res, 2004
Silicon (2) ,[object Object],Gogotsi, J Mater Res, 2004
Silicon (3) ,[object Object],[object Object],1 mN/s 5 mN/s Gogotsi, J Mater Res, 2004
Silicon (4) ,[object Object],[object Object],[object Object],Gogotsi, J Mater Res, 2004
Germanium (1) ,[object Object],[object Object],[object Object],Pharr, APL, 2005
Germanium (2) ,[object Object],[object Object],[object Object],Pharr, APL, 2005
Thin Film and MEMS Structure – Mechanical Properties
MEMS structure (1) ,[object Object],[object Object],[object Object],[object Object],Li, Ultramicroscopy, 2003
MEMS structure (2) ,[object Object],[object Object],Lee, J Kor Ceram Soc, 2003
Thin films – Al (1) ,[object Object],[object Object],[object Object],Moris Jr, J Mater Res, 2004
Thin films – Al (2) ,[object Object],[object Object],Moris Jr, J Mater Res, 2004
Thin films – Al (3) Before indentation After indentation  with same direction After indentation  with tilted direction (dislocation in entire grain) Moris Jr, J Mater Res, 2004
Residual stress (1) ,[object Object],[object Object],[object Object],[object Object],Suresh, Acta Mater, 1998
Residual stress (2) ,[object Object],[object Object],Suresh, Acta Mater, 1998
Residual stress (3) ,[object Object],Suresh, Acta Mater, 1998
Superlattice (1) ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],Scott, MRS bulletin, 2003
Superlattice (2) ,[object Object],Scott, MRS bulletin, 2003
Biomechanics
Dental hard tissue (1) Anisotropic structure of enamel Swain, J Mater Res, 2006
Dental hard tissue (1) ,[object Object],[object Object]
Dental hard tissue (3) ,[object Object]
Dental hard tissue (4) Weihs, Archives of Oral Biology, 2002 Nanoindentation mapping of enamel tooth structure Lingual Buccal Pulp Dentin Hardness (GPa) 2.5 3 3.5 4.0 4.5 5 5.5 6 Lingual Buccal Pulp Dentin Elastic Modulus (GPa) 110 100 90 80 70 60 50 120
Human bone (1) ,[object Object],Goldstein, J Biomech, 1999
Human bone (2) ,[object Object],[object Object],Goldstein, J Biomech, 1999
Biocomposite (1) ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],Marcolongo, IEEE Bioeng, 2004
Biocomposite (2) ,[object Object],[object Object],[object Object],[object Object],Marcolongo, IEEE Bioeng, 2004
Biocomposite (3) ,[object Object],Marcolongo, IEEE Bioeng, 2004
Biocomposite (4) ,[object Object],Marcolongo, IEEE Bioeng, 2004
Newly Developed Technique
Cross-section of indentation damage(1)  Indentation Pt Fast mill Tilt Markers Slow mill Lift-off Bradby, 2004 ,[object Object]
Cross-section of indentation damage(2)  Fast unloading Slow unloading Slip line Misc. defect Extended defect Bradby, 2004 Silicon
Cross-section of indentation damage(3) GaAs InP Bradby, 2004
Cross-section of indentation damage(4) GaN ZnO Bradby, 2004
In-situ nanoindentation in SEM (1) Utke, 2006
In-situ nanoindentation in SEM (2) ,[object Object],Partial correlation between shear band formation and displacement burst in P-h curve. Utke, 2006
In-situ nanoindentation in SEM (3) ,[object Object],Utke, 2006
In-situ nanoindentation in SEM (4) Silicon pillar Median crack Basal crack Buckling Utke, 2006
In-situ nanoindentation in TEM (1) Minor, 2002
In-situ nanoindentation in TEM (2) Minor, 2002
In-situ nanoindentation in TEM (3) Before After Minor, 2002
Concluding remarks ,[object Object]

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Nano Indentation Lecture2