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Specimenprep

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TEM Specimen Preparation By Nibiao Zheng
Introduction ,[object Object],[object Object],[object Object],[object Object],[object Object]
Tem preparation methods ,[object Object],[object Object],[object Object]
Powder specimen ,[object Object],[object Object],[object Object],[object Object]
Plan-view specimens ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object]
Locally electropolishing ,[object Object],Anode electrolyte Copper wire specimen beaker Good for material that can’t be prepared by mechanical method. But the electrolyte needs H 3 PO 4 , which is easy to explode - need to be in cooling environment. Good for conventional TEM, not quite suitable for HRTEM Cathode
Cross-section specimens ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object]
Notes for mechanical thinning ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object]
Notes for operation of PIPS ,[object Object],[object Object],[object Object],[object Object],[object Object]
Focused Ion beam (FIB) ,[object Object],[object Object],[object Object],[object Object],[object Object]
Procedure of FIB a. Select an area of interest, Coat with a layer of metal (Pt) b. Make “trench” using high current ion beam c. Thinning the wall d. Cut the wall and remove
Lithography ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object]
Ultramicrotomy ,[object Object],[object Object],[object Object],[object Object]
Preferential chemical etching ,[object Object]
Other methods ,[object Object],[object Object],[object Object]
Contamination of TEM specimens ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object]

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Specimenprep

  • 1. TEM Specimen Preparation By Nibiao Zheng
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  • 11. Procedure of FIB a. Select an area of interest, Coat with a layer of metal (Pt) b. Make “trench” using high current ion beam c. Thinning the wall d. Cut the wall and remove
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