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Filtration
Filtration
• Filtration is the mechanical or physical
  operation which is used for the separation of
  solids from fluids (liquids or gases)
• Uses a medium through which only the fluid
  can pass.
• Oversize solids in the fluid are retained,
• filtrate may contain some fine particles
     • depending on the pore size
• The separation of solids
Liquid Filtration
                      from a suspension in a
                      liquid by means of a porous
                      medium or screen which
                      retains the solids and
                      allows the liquid to pass is
                      termed filtration.
Important parameters to be
      considered for liquid filtration
(a) The properties of the fluid, particularly its
  viscosity, density and corrosive properties.
(b) The nature of the solid—its particle size and
  shape, size distribution, and packing
characteristics.
(c) The concentration of solids in suspension.
(d) The quantity of material to be handled, and
  its value.
Important parameters to be
      considered for liquid filtration
e) Whether the valuable product is the solid, the
   fluid, or both.
(f) Whether it is necessary to wash the filtered
   solids.
(g) Whether very slight contamination caused by
   contact of the suspension or filtrate
with the various components of the equipment is
   detrimental to the product.
(i) Whether any form of pretreatment might be
   helpful.
Liquid Filtration
• Filtration is essentially a mechanical operation
  and is less demanding in energy than evaporation
  or drying where the high latent heat of water is to
  be provided.
• In Filtration, the cake gradually builds up on the
  medium and the resistance to flow progressively
  increases.
• During the initial period of flow, particles are
  deposited in the surface layers of the cloth to
  form the true filtering medium.
Factors on which rate of filtration
               depends
(a) The drop in pressure from the feed to the far
  side of the filter medium.
(b) The area of the filtering surface.
(c) The viscosity of the filtrate.
(d) The resistance of the filter cake.
(e) The resistance of the filter medium and
  initial layers of cake.
Types of Filtration
• Cake Filtration
• Deep Bed Filtration
Cake Filtration
• particles from the suspension, which usually has
  a high proportion of solids, are deposited on the
  surface of a porous septum which should ideally
  offer only a small resistance to flow.
• As the solids build up on the septum, the initial
  layers form the effective filter medium,
• It prevents the particles from embedding
  themselves in the filter cloth
• Also ensures that a particle-free filtrate is
  obtained.
Deep Bed Filtration
• particles penetrate into the pores of the filter
  medium,
• used for the removal of fine particles from very
  dilute suspensions
• Recovery of the particles is not of primary
  importance.
• Filter bed becomes clogged with particles
• Resistance to flow increases (Very high)
• Removal of accumulated solids is necessary
Filter Medium
• The function of the filter medium is generally
  to act as a support for the filter cake
• the initial layers of cake provide the true filter.
• The filter medium should be mechanically
  strong, resistant to the corrosive action of the
  fluid
• offer as little resistance as possible
Filter Medium
• Woven materials are commonly
• the ease of cake removal
• since this is a key factor in the operation of
  modern automatic units
Filtration Theory and Mechanism
• Defined as rate of flow of a fluid through a
  bed of granular material given in Chapter 4,
  Vol 2 Rich. And Coulson
• Though some differences may occur (as due to
  increase in filter cake height)
• However generalization can be made
Filtration Theory and
Mechanism
where V is the volume of filtrate which
has passed in time t ,
A is the total cross-sectional area of
the filter cake,
uc is the average/superficial velocity of
the filtrate,
l is the cake thickness
S is the specific surface of the particles,
e is the voidage,
μ is the viscosity of the filtrate,
and P is the applied pressure
difference.
Filtration Theory and
Mechanism
Equation can be simplified to :
Relation between thickness of
 cake and volume of filtrate
Relation between thickness of
 cake and volume of filtrate
Filter selection
• one which will fulfils the requirements at
  minimum overall cost.
• Filtering area
     • obtain a high overall rate of filtration.
     • use of relatively high pressures
     • But max pressures are often limited by mechanical
       design
• Higher throughput obtained from a
  continuous filter than from a batch filter
  – But continuous operate under reduced Pressure
Filter selection
•   Quality of Filtrate
•   specific resistance of the filter cake
•   quantity to be filtered
•   solids concentration
Types of Filters
• Bag Filters
• Plate and frame press
• Pressure leaf filters
     • Cartridge filters
• Vacuum Filter
• Rotary Drum Filter
Filtration

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Filtration

  • 2. Filtration • Filtration is the mechanical or physical operation which is used for the separation of solids from fluids (liquids or gases) • Uses a medium through which only the fluid can pass. • Oversize solids in the fluid are retained, • filtrate may contain some fine particles • depending on the pore size
  • 3. • The separation of solids Liquid Filtration from a suspension in a liquid by means of a porous medium or screen which retains the solids and allows the liquid to pass is termed filtration.
  • 4. Important parameters to be considered for liquid filtration (a) The properties of the fluid, particularly its viscosity, density and corrosive properties. (b) The nature of the solid—its particle size and shape, size distribution, and packing characteristics. (c) The concentration of solids in suspension. (d) The quantity of material to be handled, and its value.
  • 5. Important parameters to be considered for liquid filtration e) Whether the valuable product is the solid, the fluid, or both. (f) Whether it is necessary to wash the filtered solids. (g) Whether very slight contamination caused by contact of the suspension or filtrate with the various components of the equipment is detrimental to the product. (i) Whether any form of pretreatment might be helpful.
  • 6. Liquid Filtration • Filtration is essentially a mechanical operation and is less demanding in energy than evaporation or drying where the high latent heat of water is to be provided. • In Filtration, the cake gradually builds up on the medium and the resistance to flow progressively increases. • During the initial period of flow, particles are deposited in the surface layers of the cloth to form the true filtering medium.
  • 7. Factors on which rate of filtration depends (a) The drop in pressure from the feed to the far side of the filter medium. (b) The area of the filtering surface. (c) The viscosity of the filtrate. (d) The resistance of the filter cake. (e) The resistance of the filter medium and initial layers of cake.
  • 8. Types of Filtration • Cake Filtration • Deep Bed Filtration
  • 9. Cake Filtration • particles from the suspension, which usually has a high proportion of solids, are deposited on the surface of a porous septum which should ideally offer only a small resistance to flow. • As the solids build up on the septum, the initial layers form the effective filter medium, • It prevents the particles from embedding themselves in the filter cloth • Also ensures that a particle-free filtrate is obtained.
  • 10. Deep Bed Filtration • particles penetrate into the pores of the filter medium, • used for the removal of fine particles from very dilute suspensions • Recovery of the particles is not of primary importance. • Filter bed becomes clogged with particles • Resistance to flow increases (Very high) • Removal of accumulated solids is necessary
  • 11. Filter Medium • The function of the filter medium is generally to act as a support for the filter cake • the initial layers of cake provide the true filter. • The filter medium should be mechanically strong, resistant to the corrosive action of the fluid • offer as little resistance as possible
  • 12. Filter Medium • Woven materials are commonly • the ease of cake removal • since this is a key factor in the operation of modern automatic units
  • 13. Filtration Theory and Mechanism • Defined as rate of flow of a fluid through a bed of granular material given in Chapter 4, Vol 2 Rich. And Coulson • Though some differences may occur (as due to increase in filter cake height) • However generalization can be made
  • 14. Filtration Theory and Mechanism where V is the volume of filtrate which has passed in time t , A is the total cross-sectional area of the filter cake, uc is the average/superficial velocity of the filtrate, l is the cake thickness S is the specific surface of the particles, e is the voidage, μ is the viscosity of the filtrate, and P is the applied pressure difference.
  • 16. Relation between thickness of cake and volume of filtrate
  • 17. Relation between thickness of cake and volume of filtrate
  • 18. Filter selection • one which will fulfils the requirements at minimum overall cost. • Filtering area • obtain a high overall rate of filtration. • use of relatively high pressures • But max pressures are often limited by mechanical design • Higher throughput obtained from a continuous filter than from a batch filter – But continuous operate under reduced Pressure
  • 19. Filter selection • Quality of Filtrate • specific resistance of the filter cake • quantity to be filtered • solids concentration
  • 20. Types of Filters • Bag Filters • Plate and frame press • Pressure leaf filters • Cartridge filters • Vacuum Filter • Rotary Drum Filter